Reaction of lithium 2,3,4,5-tetramethylphopholide with MCl3 gives η5-(C4Me4P)2·MCl·LiCl·(solvent)2[solvent = Et2O,1,2-dimethoxyethane (DME), M = Y, Lu], which are the first reported π-heterocyclopentadienyl compounds of group 3 metals.
F. Nief and F. Mathey, J. Chem. Soc., Chem. Commun., 1989, 800 DOI: 10.1039/C39890000800
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