SCHEDULED MAINTENANCE
The reaction of organic nitriles with (NSCl)3 at 23 °C, preferably under u.v. irradiation, produces the six-membered rings RCN3S2Cl2(R = But, CCl3, Me2N, Et2N, Pr2iN), which are converted to the five-membered rings RCN2S2+Cl– upon mild thermolysis.
A. Apblett and T. Chivers, J. Chem. Soc., Chem. Commun., 1989, 96 DOI: 10.1039/C39890000096
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