SCHEDULED MAINTENANCE
Nitration of iodobenzene, o-iodotoluene, and p-iodotoluene in acetic anhydride results in reversible oxidation to aryliodine(III) compounds prior to the formation of the expected nitro derivatives. µ-Oxo-[nitrato(phenyl)iodine][phenyl(trifluoroacetato)iodine] has been isolated from nitration of iodobenzene and its crystal structure determined.
G. W. Bushnell, A. Fischer and P. N. Ibrahim, J. Chem. Soc., Perkin Trans. 2, 1988, 1281 DOI: 10.1039/P29880001281
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