A new and totally general method for the determination of the hyperfine coupling tensors from the ENDOR spectra of polycrystalline samples is presented. The tensor for the γ-proton of the complex bis(pentane-2,4-dionato)oxovanadium(IV) is extracted by fitting the experimental variation of the hyperfine splitting to that calculated from theory.
G. J. Baker and J. B. Raynor, J. Chem. Soc., Faraday Trans. 1, 1988, 84, 4267 DOI: 10.1039/F19888404267
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