The molecular structure of the oxygen–sulphur exchange reagent [PhSP(S)S]2 has been determined by X-ray diffraction. It is monoclinic, space group P21/n, with a= 6.410(1), b= 11.701 (3), c= 11.409(2)Å, β= 101.92(2)°, Z= 2, and R= 0.044 for 1 473 unique observed reflections.
M. Yokoyama and K. Ogata, J. Chem. Soc., Dalton Trans., 1988, 2225 DOI: 10.1039/DT9880002225
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