The combined use of 13C and 17O spin–lattice relaxation times for co-ordinated carbonyl ligands in [M3(CO)12] clusters (M = Fe, Ru, or Os) allows the determination of 17O quadrupolar coupling constants and the correlation times for molecular tumbling at different temperatures.
S. Aime, M. Botta, R. Gobetto and D. Osella, J. Chem. Soc., Dalton Trans., 1988, 791 DOI: 10.1039/DT9880000791
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