The compounds Os6(CO)18(O2CCF3)2(1) and Os4(CO)12(O2CCF3)2(2), isolated in low yields from the reaction of Os6(CO)18 with Hg(O2CCF3)2, have been found by X-ray analysis to have unusual planar arrangements of the metal atoms.
M. P. Diebold, S. R. Drake, B. F. G. Johnson, J. Lewis, M. McPartlin and H. Powell, J. Chem. Soc., Chem. Commun., 1988, 1358 DOI: 10.1039/C39880001358
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