The xylose–mannose and xylose–glucose carbon-linked disaccharides 7 and 9 have been synthesised by a sequence in which the key steps are face selective 1,3-dipolar cycloaddition of xylose nitrile oxide (1) to the glucose-derived alkene (2) and reductive hydrolytic cleavage of the resulting 2-isoxazolines.
I. M. Dawson, T. Johnson, R. M. Paton and R. A. C. Rennie, J. Chem. Soc., Chem. Commun., 1988, 1339 DOI: 10.1039/C39880001339
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