N(1)-Phospho-L-tryptophan was prepared by phosphorylation with dimethyl phosphorochloridate of benzyl Nα-(benzyloxycarbonyl)-N(1)-lithiotryptophanate followed by deprotection with CF3SO3H–CF3CO2H–Me2S–m-cresol.
H. A. Guillaume, J. W. Perich, R. B. Johns and G. W. Tregear, J. Chem. Soc., Chem. Commun., 1988, 970 DOI: 10.1039/C39880000970
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