Mössbauer data are reported for the Li+, Na+, and K+ salts of the triphenylstannide anion; the X-ray crystal structure of Ph3SnK(18-crown-6) shows that the triphenylstannide is a naked pyramidal ion (Sn–C 2.224 Å, C–Sn–C, 96.9°): no solvent molecules are incorporated into the structure.
T. Birchall and J. A. Vetrone, J. Chem. Soc., Chem. Commun., 1988, 877 DOI: 10.1039/C39880000877
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