SCHEDULED MAINTENANCE
A β-D-fructofuranose fused oxazolidine-2-thione has been isolated as the t-butyldimethylsilyl derivative (6), which when desulphurised and treated with α-amino-α-cyanoacetamide gave the silylated 1-β-D-fructofuranosyl aminoimidazole (2b) which when deblocked with methanolic hydrogen chloride produced 5-amino-β-D-fructofuranosyl-imidazole-4-carboxamide (2a).
A. Grouiller, G. Mackenzie, B. Najib, G. Shaw and D. Ewing, J. Chem. Soc., Chem. Commun., 1988, 671 DOI: 10.1039/C39880000671
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