The cation [Ir(CO)3(PEt3)2]+ reacts with XeF2 in CH2Cl2 to give the novel species [Ir(CO)2F(COF)PEt3)2]+(1), isolated as BF4– and PF6– salts and characterised spectroscopically, crystallographically, and by partial elemental analysis.
A. J. Blake, R. W. Cockman, E. A. V. Ebsworth and J. H. Holloway, J. Chem. Soc., Chem. Commun., 1988, 529 DOI: 10.1039/C39880000529
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