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Issue 0, 1987
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Phosphorus-nitrogen compounds. Part 49. The synthesis and mechanism of formation of 6-chloro-5,6,7,12-tetrahydro-2,5,7,10-tetramethyldibenzo[d,g][1,3,2]-diazaphosphocine 6-oxide and 6-sulphide

Abstract

A reaction mechanism is proposed for the formation of the title compounds in the reactions between N,Ndimethyl-p-toluidine and phosphoryl and thiophosphoryl chlorides. The synthesis of 2,2′-methylenebis(p-toluidine) and 2,2′-methylenebis(N-methyl-p-toluidine) are described, as are their reactions with phosphoryl and thiophosphoryl chlorides.

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J. Chem. Soc., Perkin Trans. 1, 1987, 1547-1552
Article type
Paper

Phosphorus-nitrogen compounds. Part 49. The synthesis and mechanism of formation of 6-chloro-5,6,7,12-tetrahydro-2,5,7,10-tetramethyldibenzo[d,g][1,3,2]-diazaphosphocine 6-oxide and 6-sulphide

T. Demir and R. A. Shaw, J. Chem. Soc., Perkin Trans. 1, 1987, 1547
DOI: 10.1039/P19870001547

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