The radical anion species [Os10C(CO)24]˙– and [Os10H4(CO)24]˙– have been prepared by electrochemical and chemical methods (AgBF4–CH2Cl2 or FeCl3–tetrahydrofuran); as expected they are paramagnetic and exhibit strong signals in their e.s.r. spectra.
S. R. Drake, B. F. G. Johnson, J. Lewis and R. C. S. McQueen, J. Chem. Soc., Dalton Trans., 1987, 1051 DOI: 10.1039/DT9870001051
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