The Raman and i.r. spectra of [Ni(CO)3(SbCl3)] are reported for the first time. A complete vibrational assignment is made, consistent with C3v molecular symmetry. The wavenumber of the nickel–antimony stretching vibration is ca. 230 cm–1.
H. G. M. Edwards, J. Chem. Soc., Dalton Trans., 1987, 681 DOI: 10.1039/DT9870000681
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