The novel reagent NSCl3 is readily generated by treatment of (NSCl)3 with an excess of SO2Cl2; the reactions of NSCl3 with methacrylonitirle or thioacetamide produce 4-cyanosiothiazole or 5-methyl-1,3,2,4-dithiazolium chloride, respectively, in good yields.
A. Apblett and T. Chivers, J. Chem. Soc., Chem. Commun., 1987, 1889 DOI: 10.1039/C39870001889
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