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A single crystal X-ray structural analysis reveals that black cubes of Cs3Mo4P3O16, synthesized from Cs2MoO4, MoO3, Mo, and P2O5 at 950 °C, contain isolated Mo4O46+ cubes, with six short Mo–Mo bonds, with the cubes bridged together into a three dimensional array by PO43– groups.
R. C. Haushalter, J. Chem. Soc., Chem. Commun., 1987, 1566 DOI: 10.1039/C39870001566
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