Base hydrolysis of (η5-C5Me5)TiCl3 in toluene yields [(η5-C5Me5)Ti]4O6 which, according to X-ray structural analysis, has an adamantane-like cage structure with a tetrahedral TiIV4O6 core.
L. M. Babcock, V. W. Day and W. G. Klemperer, J. Chem. Soc., Chem. Commun., 1987, 858 DOI: 10.1039/C39870000858
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