The hypervalent iodine oxidative decarboxylation of homocubyl and cubyl mono- and di-carboxylic acids is reported; the carboxylic acid is treated with Phl(OAc)2–CCl4–I2 under irradiation conditions and 80–90% of the derived iodo compound is obtained.
R. M. Moriarty, J. S. Khosrowshahi and T. M. Dalecki, J. Chem. Soc., Chem. Commun., 1987, 675 DOI: 10.1039/C39870000675
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