The first solid-state carbon-13 magic-angle sample-spinning n.m.r. spectra of an antiferromagnetically-coupled species, [Cu(HCO2)2(C5H5N)]2 are reported, the results indicating that essentially diamagnetic behaviour can be observed at –180 °C, while increasing temperature results in a shifted and progressively broadened resonance, owing to spin unpairing.
T. H. Walter and E. Oldfield, J. Chem. Soc., Chem. Commun., 1987, 646 DOI: 10.1039/C39870000646
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