Exposure of trimethylsilylacetylene and bis(trimethylsilyl)acetylene to positive muons gave radicals whose muon–electron hyperfine coupling constants establish that the corresponding vinyl radicals were formed.
C. J. Rhodes, M. C. R. Symons, C. A. Scott, E. Roduner and M. Heming, J. Chem. Soc., Chem. Commun., 1987, 447 DOI: 10.1039/C39870000447
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