Bisacetylacetonato-oxovanadium [VO(acac)2] is a selective reagent for the quantitative cleavage of ditertiary glycols, under mild conditions. The reaction takes place also with catalytic amounts of the reagent in the presence of t-butyl hydroperoxide or m-chloroperbenzoic acid.
M. Zviely, A. Goldman, I. Kirson and E. Glotter, J. Chem. Soc., Perkin Trans. 1, 1986, 229 DOI: 10.1039/P19860000229
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