Reaction of (NMe4)2WS4 with CuCl and KSCN (1 : 2 : 2) in CH3CN–CH2Cl2(1 : 1) produces the bimetallic sulphur anion; a crystal structure determination shows that four edges of the WS4Cu4 core are –NCS–bridged giving a three-dimensional polymer.
J. M. Manoli, C. Potvin, F. Secheresse and S. Marzak, J. Chem. Soc., Chem. Commun., 1986, 1557 DOI: 10.1039/C39860001557
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