Vinylphosphine (1) has been synthesized from diethyl vinylphosphonate in three steps including a retro cycloaddition reaction using flash vacuum pyrolysis (overall yield ∼30%) and characterized by mass, i.r., and n.m.r. spectroscopy; it exhibits a remarkable stability at room temperature in neutral solution.
M. Lasne, J. Ripoll and A. Thuillier, J. Chem. Soc., Chem. Commun., 1986, 1428 DOI: 10.1039/C39860001428
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