The electrochemical preparation and characterisation in terms of oxidation state, spectra, stability, and reduction potentials of IrIV and IrV aqua ions in 2 M HClO4, and related binuclear IrIII ions, is described.
S. E. Castillo-Blum, D. T. Richens and A. G. Sykes, J. Chem. Soc., Chem. Commun., 1986, 1120 DOI: 10.1039/C39860001120
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