SCHEDULED MAINTENANCE
Heating thiophosphinate O-esters and thiophosphinamides having the 7-phosphanorbornene framework results in elimination of fragments that are derivatives of thiophosphenous O-acid; they are trapped by cycloaddition with 2,3-dimethylbutadiene to form 2,5-dihydrophospholes.
L. D. Quin and J. Szewczyk, J. Chem. Soc., Chem. Commun., 1986, 844 DOI: 10.1039/C39860000844
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