The reaction of [(Me3P)3H3W(µ-H)2AlH(µ-H)]2 with lithium alkyls in diethyl ether yields the bright yellow complex {[(Me3P)3WH5]–Li+}4 whose structure has been determined by X-ray crystallography and nuclear magnetic resonance spectroscopy; the complex has high solubility and stability in organic solvents.
A. R. Barron, M. B. Hursthouse, M. Motevalli and G. Wilkinson, J. Chem. Soc., Chem. Commun., 1986, 81 DOI: 10.1039/C39860000081
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