The compounds M(O2PF2)2·HPO2F2(M = Mn, Fe, Co, or Ni), Cr(O2PF2)3·HPO2F2, and two new forms of Fe(O2PF2)3 have been prepared and characterised by elemental analysis, i.r. spectroscopy, magnetic measurements [M(O2PF2)2·HPO2F2], and Móssbauer spectroscopy (iron compounds). All the compounds appear to be polymeric with bidentate bridging difluorophosphate groups and the metal atoms in octahedral environments.
M. F. A. Dove, R. C. Hibbert and N. Logan, J. Chem. Soc., Dalton Trans., 1985, 707 DOI: 10.1039/DT9850000707
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