Dianions from t-butyl acetothioacetate may be alkylated at the γ-carbon atom with suitably protected iodoalkanols to afford useful precursors for dimerisation to novel bis-β-ketomacrolides in the presence of copper(I) trifluoroacetate.
C. M. J. Fox, S. V. Ley, A. M. Z. Slawin and D. J. Williams, J. Chem. Soc., Chem. Commun., 1985, 1805 DOI: 10.1039/C39850001805
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