Chemistry of bacterial endotoxins. Part 2. A practical synthesis of 6-O-{4-O-ammonio(hydrogen)phosphono-2-deoxy-2-[(3R)-3-hydroxytetradecanamido]-β-D-glucopyranosyl}-2-deoxy-2-[(3R)-3-hydroxytetradecanamido]-D-glucose
Abstract
An improved method for the preparation of the phosphorylated disaccharide named in the title, via benzyl 2-amino-6-O-(2-amino-2-deoxy-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranoside, is described.