SCHEDULED MAINTENANCE
A facile and efficient synthesis of (–)-cherylline (1) was accomplished in 46% overall yield starting from the readily accessible (12S)-(–)-3,9-dibenzyloxy-2-methoxy-tetrahydro-6,12-methanodibenz[c.f]azocine (4)viaa regiocontrolled Polonovski-type reaction as the key step.
T. Nomoto, N. Nasui and H. Takayama, J. Chem. Soc., Chem. Commun., 1984, 1646 DOI: 10.1039/C39840001646
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