A two-dimensional n.m.r. experiment correlating proton and deuterium chemical shift resonances has been developed to reveal the precise location of deuterium labels; this technique can be used to edit a 2H n.m.r. spectrum when overlapping resonances prevent assignments of a one-dimensional spectrum.
S. J. Gould, V. A. Palaniswamy, H. Bleich and J. Wilde, J. Chem. Soc., Chem. Commun., 1984, 1075 DOI: 10.1039/C39840001075
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