Issue 14, 1984
From the journal:

Journal of the Chemical Society, Chemical Communications

The high yield synthesis of an unsaturated osmium cluster; the X-ray crystal structure of [Os3(CO)8(H){Ph2PCH2P(Ph)C6H4}]

Jennifer A. Clucas,   Douglas F. Foster,   Marjorie M. Harding  and  Anthony K. Smith  

Abstract

Thermolysis of [Os3(CO)10(dppm)](dppm = Ph2PCH2PPh2) in refluxing toluene affords a high yield of the unsaturated cluster [Os3(CO)8(H){Ph2PCH2P(Ph)C6H4}] which has been characterized by X-ray crystallography, and which undergoes a facile reversible reaction with CO.

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Article information

DOI
https://doi.org/10.1039/C39840000949
Article type
Paper

J. Chem. Soc., Chem. Commun., 1984, 949-950

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The high yield synthesis of an unsaturated osmium cluster; the X-ray crystal structure of [Os3(CO)8(H){Ph2PCH2P(Ph)C6H4}]

J. A. Clucas, D. F. Foster, M. M. Harding and A. K. Smith, J. Chem. Soc., Chem. Commun., 1984, 949 DOI: 10.1039/C39840000949

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