Issue 13, 1984

Confirmation of a short intramolecular C–H ⋯ N hydrogen bond in 4,4-bisphenylsulphonyl-2,N,N-trimethylbutylamine by X-ray crystallography

Abstract

The X-ray crystal structure of the title compound, (3), reveals a close intramolecular contact between the polar methine hydrogen and amino nitrogen atoms of 2.34(3)Å, consistent with the hydrogen bonding interaction detected in solution by 1H n.m.r. spectroscopy.

Article information

Article type
Paper

J. Chem. Soc., Chem. Commun., 1984, 818-819

Confirmation of a short intramolecular C–H ⋯ N hydrogen bond in 4,4-bisphenylsulphonyl-2,N,N-trimethylbutylamine by X-ray crystallography

R. L. Harlow, C. Li and M. P. Sammes, J. Chem. Soc., Chem. Commun., 1984, 818 DOI: 10.1039/C39840000818

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