A stable phosphinous acid complex, H2P(OH)W(CO)5, was prepared by LiAlH4 reduction followed by acid hydrolysis of the corresponding diethylaminodichlorophosphine complex.
F. Mercier and F. Mathey, J. Chem. Soc., Chem. Commun., 1984, 782 DOI: 10.1039/C39840000782
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