Tertiary alcohols can be dexygenated in a radical chain reaction based on their mixed oxalate esters with N-hydroxy-2-thiopyridone, these esters being obtained directly from the alcohols and chloride etc, or via their trimethylsilyl derivatives.
D. H. R. Barton and D. Crich, J. Chem. Soc., Chem. Commun., 1984, 774 DOI: 10.1039/C39840000774
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