A high yield synthesis of tetraselenafulvalene (TSF) involving a novel acid catalysed exchange reaction between diselenides and bis(N,N-dialkyselenocarbamoyl)selenides is reported.
I. Johannsen, K. Lerstrup, L. Henriksen and K. Bechgaard, J. Chem. Soc., Chem. Commun., 1984, 89 DOI: 10.1039/C39840000089
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