The insect pheromone (+)-exo-brevicomin (9) has been synthesised from the methyl 6-deoxy-6-iodo-α-D-glucopyranoside derivative (1) in 54% yield by way of the dienone (5) from which the ketone (7) was obtained by concurrent hydrogenation of the double bonds and hydrogenolysis of the allylic ester group.
R. J. Ferrier and P. Prasit, J. Chem. Soc., Perkin Trans. 1, 1983, 1645 DOI: 10.1039/P19830001645
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