An improved synthesis of the (±)-limaspermine intermediate (3b), starting from tricarbonyl-1—4-η-[4-isopropoxy-1-(2-methoxyethyl)cyclohexa-1,3-diene]iron (2c), is described.
A. J. Pearson, D. C. Rees and C. W. Thornber, J. Chem. Soc., Perkin Trans. 1, 1983, 619 DOI: 10.1039/P19830000619
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