Condensation of 2,3,4,6-tetrabenzylglucopyranolactone with the anion of methyl 6,7-dideoxy-2,3,4-tri-O-benzyl-α-D-gluco-hept-6-ynopyranoside followed by triethylsilane reduction provided, after hydrogenolysis, the first example of a synthetic β(1 → 6′)-‘C-disaccharide.’
D. Rouzaud and P. Sinaÿ, J. Chem. Soc., Chem. Commun., 1983, 1353 DOI: 10.1039/C39830001353
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