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An initially homogeneous solution of hydroxylamine in nitric acid can react to form a two-layer system, a layer of nitrous acid in nitric acid above a lawyer of hydroxylamine in nitric acid, with a sharp boundary between them that moves steadily downwards.
R. J. Gowland and G. Stedman, J. Chem. Soc., Chem. Commun., 1983, 1038 DOI: 10.1039/C39830001038
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