Ethoxycarbonylmethanesulphenyl chloride reacts with triethylamine to give the transient thioaldehyde, ethyl thioxoacetate, which has been trapped, in situ, by cycloaddition to various conjugated dienes.
C. M. Bladon, I. E. G. Ferguson, G. W. Kirby, A. W. Lochead and D. C. McDougall, J. Chem. Soc., Chem. Commun., 1983, 423 DOI: 10.1039/C39830000423
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