It is shown by i.r. spectroscopy, using mixtures of 12CO and 13CO, that isolated Ni+ ions produced by u.v. irradiation in hydrogen at 77 K of an Ni-exchanged silica can form mono- or di-carbonyl adducts in the 10–5–5 Torr range.
M. Kermarec, D. Delafosse and M. Che, J. Chem. Soc., Chem. Commun., 1983, 411 DOI: 10.1039/C39830000411
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