Partial deuteriation of exchangeable hydroxy-protons in carbohydrates produces characteristic multiplets in 13C n.m.r. spectra observed under slow exchange conditions, enabling most carbon signals to be assigned unequivocally in one experiment by analysis of two and three bond isotope effects.
J. C. Christofides and D. B. Davies, J. Chem. Soc., Chem. Commun., 1983, 324 DOI: 10.1039/C39830000324
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