Reaction of the ditopic hexa-aza-macrocycle (1) with tetracarbonyldichlorodirhodium(I) yields the dinuclears rhodium–carbonyl complex (1)–Rh2, which may be considered as a cryptate of triply bridged [Rh(CO)3Rh]2+ unit held inside the intramolecular cavity of the ligand.
J. Lecomte, J. Lehn, D. Parker, J. Guilhem and C. Pascard, J. Chem. Soc., Chem. Commun., 1983, 296 DOI: 10.1039/C39830000296
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