The flash vacuum thermolysis and/or gas–solid phase multistep sequences allow the synthesis of vinylideneamine and a safe, preparative-scale synthesis of Δ1-azirine.
J. Guillemin, J. Denis, M. Lasne and J. Ripoll, J. Chem. Soc., Chem. Commun., 1983, 238 DOI: 10.1039/C39830000238
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