Treatment of triphenylphosphine with diethyl azodicarboxylate and hydrogen peroxide results in the formation of phenyl diphenylphosphinate; triphenylphosphine dioxide is suggested as an intermediate.
M. von Itzstein and I. D. Jenkins, J. Chem. Soc., Chem. Commun., 1983, 164 DOI: 10.1039/C39830000164
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