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Issue 5, 1982
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Crystal structure of 1-(mesityl-2-sulphonyl)-3-nitro-1,2,4-triazole

Abstract

The crystal structure of 1-(mesityl-2-sulphonyl)-3-nitro -1,2,4-triazole (1a) has been determined from three-dimensional diffractometer data. The triclinic unit cell, P[1 with combining macron], has dimensions a= 8.001(1), b= 8.140(2), c= 12.892(1)Å, α= 98.22(1)°, β= 105.49(1)°, γ= 102.12(1)°, and Z= 2. The structure was solved by the heavy atom method and refined to R 0.0736 for 2 926 reflections (Fo > 3σFo). The crystal structure confirms that the product of reaction of 3-nitrotriazole and mesitylenesulphonyl chloride is 1-(mesityl-2-sulphonyl)-3-nitro-1,2,4-triazole.

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Article type: Paper
DOI: 10.1039/P29820000617
Citation: J. Chem. Soc., Perkin Trans. 2, 1982,0, 617-620

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    Crystal structure of 1-(mesityl-2-sulphonyl)-3-nitro-1,2,4-triazole

    R. Kuroda, M. R. Sanderson, S. Neidle and C. B. Reese, J. Chem. Soc., Perkin Trans. 2, 1982, 0, 617
    DOI: 10.1039/P29820000617

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