The synthesis is described of 2,5-dihydroxy-3-(4-hydroxybenzyl)-6-methylpyrazine 1,4-dioxide (9), an isomer of degeranylmycelianamide (7), starting with 3-(4-hydroxybenzyl)-6-methylpiperidine-2,5-dione. The chemistry of the dioxide (9) has been explored; acetylation of this compound and of degeranylmycelianamide has been shown to afford the same product.
A. K. Göktürk, A. A. E. Porter and P. G. Sammes, J. Chem. Soc., Perkin Trans. 1, 1982, 953 DOI: 10.1039/P19820000953
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