The formation of [Ni(pc)](pc = phthalocyaninate) through the stepwise reactions of nickel ion and phthalonitrile in a two-compartment electrolyzer separated with an ion-exchange membrane is traced. Five reaction intermediates, which readily convert to [Ni(pc)] upon heating, were isolated by means of preparative thin-layer chromatography and characterised mass spectrometrically.
C. H. Yang and C. Chang, J. Chem. Soc., Dalton Trans., 1982, 2539 DOI: 10.1039/DT9820002539
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